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Glycerin-assisted solvothermal synthesis of Fe3(PO4)2(OH)2microspheres
Yu, Ya-Dong1,2; Zhu, Ying-Jie1,2; Wu, Jin1
2017
Source PublicationMaterials Letters
ISSN0167577X
Volume205Pages:158-161
AbstractIron hydroxyl phosphate (Fe3(PO4)2(OH)2) microspheres with diameters of several micrometers have been successfully prepared using Fe(NO3)3·9H2O and NaH2PO4·2H2O in a mixed solvent of deionized water and glycerin by a facile one-step solvothermal method. The crystal phase of the product changes from poorly crystallized FePO4·2H2O nanoparticles into well-crystallized Fe3(PO4)2(OH)2microspheres as the amount of glycerin increases. The as-prepared Fe3(PO4)2(OH)2microspheres can transform into FePO4through thermal treatment at 800 °C in air. The cytotoxicity tests show that the as-prepared Fe3(PO4)2(OH)2microspheres have good biocompatibility. We expect that the as-prepared Fe3(PO4)2(OH)2microspheres are promising for the applications in various fields. © 2017 Elsevier B.V.
DOI10.1016/j.matlet.2017.06.071
EI Accession Number20172603813480
EI KeywordsIron compounds
EI Classification Number445.1 Water Treatment Techniques - 461.9.1 Immunology - 462.5 Biomaterials (including synthetics) - 804.1 Organic Compounds - 951 Materials Science
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Cited Times:1[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.sic.ac.cn/handle/331005/25761
Collection中国科学院上海硅酸盐研究所
Affiliation1.State Key Laboratory of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai; 200050, China;
2.University of Chinese Academy of Sciences, Beijing; 100049, China
Recommended Citation
GB/T 7714
Yu, Ya-Dong,Zhu, Ying-Jie,Wu, Jin. Glycerin-assisted solvothermal synthesis of Fe3(PO4)2(OH)2microspheres[J]. Materials Letters,2017,205:158-161.
APA Yu, Ya-Dong,Zhu, Ying-Jie,&Wu, Jin.(2017).Glycerin-assisted solvothermal synthesis of Fe3(PO4)2(OH)2microspheres.Materials Letters,205,158-161.
MLA Yu, Ya-Dong,et al."Glycerin-assisted solvothermal synthesis of Fe3(PO4)2(OH)2microspheres".Materials Letters 205(2017):158-161.
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