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Microwave aqueous synthesis of hydroxyapatite bilayer coating on magnesium alloy for orthopedic application
Shen, Sibo1,2; Cai, Shu1; Li, Yan1; Ling, Rui1; Zhang, Feiyang1; Xu, Guohua3; Wang, Fengwu1
2017
发表期刊Chemical Engineering Journal
ISSN13858947
卷号309页码:278-287
摘要Magnesium and magnesium alloys as promising biodegradable implants gain increasing interest. To improve their corrosion resistance and cytocompatibility, hydroxyapatite (HA) coatings with double-layer structure were synthesized on magnesium alloy through a rapid microwave aqueous chemical route. The coating prepared with microwave heating time of 10 min consisted of cotton-like HA as the surface layer and strip-like HA as the bottom layer, and the coating thickness was ∼10.0 μm. The growth kinetic, electrochemical property, degradation, mineralization and cytocompatibility of HA coated and naked magnesium alloys were investigated. Potentiodynamic polarization test demonstrated that corrosion current density of HA coated magnesium alloy prepared with microwave heating time of 10 min was ∼100 times lower than that of the naked counterpart. Immersion test indicated that the strip-like HA layer with thickness of ∼7.7 μm and low solubility endowed magnesium alloy with initial-stage protection; the nano-scale cotton-like HA layer exhibited high HA mineralization capacity. The mineralized layer reached ∼12.7 μm in thickness after 24 days’ immersion, eventually integrated with the original HA bilayer coating, providing favorable long-term protection for magnesium alloy. Moreover, HA coated magnesium alloy prepared with microwave heating time of 10 min enhanced osteoblast proliferation than the naked counterpart. These attractive results indicated that this HA bilayer coating is a potential protective coating on biodegradable magnesium and magnesium alloys for orthopedic application. © 2016 Elsevier B.V.
DOI10.1016/j.cej.2016.10.043
EI入藏号20164402967934
EI主题词Magnesium alloys
EI分类号482 Mineralogy - 539.1 Metals Corrosion - 542.2 Magnesium and Alloys - 711 Electromagnetic Waves - 711.1 Electromagnetic Waves in Different Media - 761 Nanotechnology - 804.2 Inorganic Compounds - 813 Coatings and Finishes - 821.4 Agricultural Products - 943.2 Mechanical Variables Measurements - 951 Materials Science
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被引频次:16[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.sic.ac.cn/handle/331005/25662
专题中国科学院上海硅酸盐研究所
作者单位1.Key Laboratory for Advanced Ceramics and Machining Technology of Ministry of Education, Tianjin University, Tianjin; 300072, China;
2.Center for Electron Microscopy, Institute for New Energy Materials & Low-Carbon Technologies, Tianjin University of Technology, Tianjin; 300384, China;
3.Shanghai Changzheng Hospital, Shanghai; 200003, China
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Shen, Sibo,Cai, Shu,Li, Yan,et al. Microwave aqueous synthesis of hydroxyapatite bilayer coating on magnesium alloy for orthopedic application[J]. Chemical Engineering Journal,2017,309:278-287.
APA Shen, Sibo.,Cai, Shu.,Li, Yan.,Ling, Rui.,Zhang, Feiyang.,...&Wang, Fengwu.(2017).Microwave aqueous synthesis of hydroxyapatite bilayer coating on magnesium alloy for orthopedic application.Chemical Engineering Journal,309,278-287.
MLA Shen, Sibo,et al."Microwave aqueous synthesis of hydroxyapatite bilayer coating on magnesium alloy for orthopedic application".Chemical Engineering Journal 309(2017):278-287.
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